|
 the
Hive BB  Methods
Discourse  MDMA
without DMF in a SRV?
|
| next newest topic | next oldest topic |
| Author | Topic: MDMA without DMF in a SRV? |
| Curiosity Junior Member |
 posted 10-06-1999 11:23 PM 
Just when I thought that my schmoozing with organic chem students paid off, I found a file on rhodium about using a soda bottle as a reaction chamber and compressing it, shaking violently, and ending with MDP2P. BONUS* this reaction doesnt use DMF! IS this reaction reliable? Could a PVC pipe vessle be used in-leu of a 2 liter coke bottle to increase safety, and this put in a paint shaker for ease of mixing? This was in a file on Rodium, by Spice Boy. I'll dig the link up if anyone would like to run with this one. If you care, could some one drop me a URL for oil at curiouskat@hushmail.com. thankx |
| Penis
Seinfeld Member |
posted 10-06-1999 11:29 PM
Are you fucking kidding me? Use the damned search engine! PS |
| Osmium Member |
posted 10-07-1999 08:37 AM
This was a very hot topic a year or so ago. Yes, it worked for me and spiceboy. KrZ claimed good yields (~90%) recently in his own variation. |
| courier Member |
posted 10-09-1999 01:16 PM
hire out a pneumatic drill to do the shaking >75% everytime. |
| Semtex
Enigma Member |
posted 10-09-1999 03:23 PM
Yeah, KRZ, still waiting for them thar Getto Reactor(TM) plans... 
As for your question(s), what your talking about is probably one of THE MOST discussed things that this board has ever seen. There should be LOADS of info floating around. And YES a paint shaker works nicely, just a question though if you don't mind. Besides an auction or a flea market, where the hell does one purchase a paint shaker??? Believe me paint stores don't wanna sell them, I guess could steal one from home depot... How did you hook it up to the pnumatic drill if you don't mind me asking? Thanks for any and all help... |
| spiceboy Member |
posted 10-11-1999 11:21 AM
If I remember correctly, during my early research I ran across the statement that DMF UNDER PRESSURE is explosive...Anyone able to verify that? Also, the shaking thing that everyone is discussing CAN be done by hand, but its certainly not the easiest way. Most recently, it has been my fortune to learn that many of my early
failures were due to the fact that I wasnt allowing enough time for the pd
to dissolve in the alcohol. A soda bottle is packaged with 45 psi of CO2 This reaction has been very quirky for many, but I have it on authority that a few bees made their first honey this way. But thers not a lot of info on it. Rhodium has most of it on his page. Peace and beans
|
| Eigenfxn Member |
posted 10-11-1999 11:23 AM
Some companies sell machines to shake cells ... check bio companies |
| Semtex
Enigma Member |
posted 10-11-1999 04:24 PM
Spicey, Baby!!! Good to see you back about... BTW SWIM heard a rumor that some idiot took a pepsi bottle up round 70psi, with no problems...
|
| Osmium Member |
posted 10-12-1999 03:36 AM
Hey spiceboy! Long time no see!
DMF is not more explosive than any other solvent under a high oxygen athmosphere. Yes, it is very important that all the Pd dissolves in the alcohol solvent before you start the reaction. One day of stirring together with the copper cocatalyst will usually accomplish that. When pressure-testing your bottle, fill it with water. When it ruptures the explosion will be much less violent this way, although it might be slightly wetter. |
|
All times are CT (US) |
next newest topic | next oldest topic |
 
|
|
Contact Us | the Hive
Powered by: Ultimate Bulletin Board, Version 5.39a
© Infopop Corporation
(formerly Madrona Park, Inc.), 1998 -
1999.